HuagongsheHuagongshe Chemistry Print Report · For research reference only
Butylamine → HCID 178449232, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Butylamine | HCID 8007 | — |
| Reactant | Methyl hydrazinecarbimidothioate hydroiodide | HCID 6508896 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 178449232 | HCID 178449232 | — |
Reaction Steps
S-Methylisothiosemicarbazide hydroiodide (46.6 g) and 1-aminobutane (48 ml) and water (100 ml) were heated under reflux for 1 hour. The resulting solution was evaporated to an oil which was crystallised from amyl alcohol/80-100 PE, to give the title compound (a).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04089962 |
| Source dataset | uspto-grants-1978_05 |
| ORD ID | ord-f2bacff0b3604575b7f45e3420a48d67 |
| Source note | uspto-grants-1978_05 |