HCID 70577452, compound → HCID 70579190, compound

HRID 372255Notes

Reaction equation

HRID 372255 reaction equation
[CH3:1][CH2:2][CH2:3][CH2:4][N:5]([C:13]1[CH:14]=[C:15]([NH:19][C:20](=[O:26])[C:21]([O:23]CC)=[O:22])[CH:16]=[CH:17][CH:18]=1)[C:6](=[O:12])[C:7]([O:9]CC)=[O:8]>[OH-].[Na+]>[CH3:1][CH2:2][CH2:3][CH2:4][N:5]([C:13]1[CH:14]=[C:15]([NH:19][C:20](=[O:26])[C:21]([OH:23])=[O:22])[CH:16]=[CH:17][CH:18]=1)[C:6](=[O:12])[C:7]([OH:9])=[O:8]

Participants

3

Reactant 1

HCID 70577452HCID 70577452, compound

Product 1

HCID 70579190HCID 70579190, compound

Reagents, catalysts & solvents 1

HCID 14798Sodium HydroxideSolvent

Procedure

Diethyl 4-butyl-N,N'-(m-phenylene)dioxamate (1.0 gm., 2.74 mmoles) is stirred at room temperature in 1.0 N NaOH (10 ml.) until the solution is complete. The solution is adjusted to pH 3 and the resulting white solid collected (0.5 gm., mp. 232°).

Workup

  1. customthe resulting white solid collected (0.5 gm., mp. 232°)

Sources & evidence

ORD record
ord-3b59a55ec1af447b90e262877eb6372a
Source dataset
uspto-grants-1978_05
Patent number
US04089973

Reaction notes

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