Acetic Anhydride → HCID 19377154, compound

HRID 372280Notes

Reaction equation

HRID 372280 reaction equation
[CH3:1][NH:2][CH:3]1[C:12]2[C:7](=[CH:8][CH:9]=[CH:10][CH:11]=2)[CH2:6][CH2:5][CH2:4]1.C(O[C:17](=[O:19])[CH3:18])(=O)C>>[C:17]([N:2]([CH:3]1[C:12]2[C:7](=[CH:8][CH:9]=[CH:10][CH:11]=2)[CH2:6][CH2:5][CH2:4]1)[CH3:1])(=[O:19])[CH3:18]

Participants

3

Reactant 2

HCID 7918Acetic AnhydrideHCID 46475N-methyl-1,2,3,4-tetrahydronaphthalen-1-amine

Product 1

HCID 19377154HCID 19377154, compound

Procedure

N-Methyl-1,2,3,4-tetrahydro-1-naphthylamine is stirred with acetic anhydride to afford N-acetyl-N-methyl-1,2,3,4-tetrahydro-1-naphthylamine, which is oxidized to N-acetyl-N-methyl-1,2,3,4-tetrahydro-4-oxo-1-naphthylamine by the method of Example 1.

Sources & evidence

ORD record
ord-a5b133e8e7444c4bb6299ebe35bdd1a4
Source dataset
uspto-grants-1978_05
Patent number
US04089976

Reaction notes

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