HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-(Trifluoromethyl)aniline → 2,2'-Dithiobis[N-[4-(trifluoromethyl)phenyl]benzamide]
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-(Trifluoromethyl)aniline | HCID 9964 | — |
| Reactant | 2,2'-Dithiodibenzoyl chloride | HCID 88164 | — |
| Solvent | Pyridine | HCID 1049 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | 2,2'-Dithiobis[N-[4-(trifluoromethyl)phenyl]benzamide] | HCID 18935295 | 24.3% |
Reaction Steps
This compound was prepared according to the general method of Example 77 using 2,2'-dithiobisbenzoyl chloride (1.12 g, 3.26 mmol) in 25 mL of dichloromethane and 4-aminobenzotrifluoride (1.05 g, 6.53 mmol) in 8 mL of pyridine. The crude product was recrystallized from water-DMF to yield 0.47 g of the title compound, mp 272°-275° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05734081 |
| Source dataset | uspto-grants-1998_03 |
| ORD ID | ord-0f7687fce75f4342a1006eb952201a30 |
| Source note | uspto-grants-1998_03 |