HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phosphorus pentachloride → HCID 13172332, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phosphorus pentachloride | HCID 24819 | — |
| Reactant | 2,4-Dichloro-3,5-dinitrobenzoic acid | HCID 96497 | — |
| Product | HCID 13172332 | HCID 13172332 | — |
Reaction Steps
A mixture of 75.0 g. (0.2669 mole) of 2,4-dichloro-3,5-dinitrobenzoic acid and 55.59 g. (0.2669 mole) of phosphorus pentachloride is heated at reflux for 90 minutes and cooled to room temperature. The phosphorus oxychloride is distilled off in vacuo. The residue is recrystallized from cyclohexane to yield 75.9 gm. (95%) of yellow needles melting at 99°-101°.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04091011 |
| Source dataset | uspto-grants-1978_05 |
| ORD ID | ord-2b2a1d6b3f7f44aa8710dea916f3f4b5 |
| Source note | uspto-grants-1978_05 |