Methylcarbamyl fluoride → N-Methyl-N-(n-Butylthiosulfenyl)Carbamoyl Fluoride

HRID 372370Notes

Reaction equation

[CH2:1]([S:5][S:6]Cl)[CH2:2][CH2:3][CH3:4].[CH3:8][NH:9][C:10]([F:12])=[O:11]>>[CH3:8][N:9]([S:6][S:5][CH2:1][CH2:2][CH2:3][CH3:4])[C:10]([F:12])=[O:11]

Participants

Reactant 2

HCID 12545956Methylcarbamyl fluoride

HCID 22748613n-Butylthiosulfenyl chloride

Product 1

HCID 20327308N-Methyl-N-(n-Butylthiosulfenyl)Carbamoyl Fluoride

Procedure

Prepared by the procedure of Example II by reacting n-butylthiosulfenyl chloride with methylcarbamoyl fluoride b.p. 68°-70° C/0.15 Torr

Workup

customPrepared by the procedure of Example II

Sources & evidence

ORD record: ord-3f58ed036c2b45c38b5cfabf3771eb21
Source dataset: uspto-grants-1978_05
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US04091016

Reaction notes

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