Acetic Anhydride → 1-Chloro-4-acetoxy-8-methylnonane

HRID 372504Notes

Reaction equation

HRID 372504 reaction equation
[Cl:1][CH2:2][CH2:3][CH2:4][CH:5]([OH:12])[CH2:6][CH2:7][CH2:8][CH:9]([CH3:11])[CH3:10].[C:13](OC(=O)C)(=[O:15])[CH3:14]>>[Cl:1][CH2:2][CH2:3][CH2:4][CH:5]([O:12][C:13](=[O:15])[CH3:14])[CH2:6][CH2:7][CH2:8][CH:9]([CH3:10])[CH3:11]

Participants

3

Reactant 2

HCID 7918Acetic AnhydrideHCID 203222521-Chloro-8-methylnonan-4-OL

Product 1

HCID 203860491-Chloro-4-acetoxy-8-methylnonane

Procedure

A mixture of 1-chloro-8-methyl-4-nonanol (22.73 g.; 0.118 mole) and acetic anhydride (24.07 g.; 0.236 mole) is heated on a steam bath for 11/2 hours.

Workup

  1. temperatureis heated on a steam bath for 11/2 hours

Sources & evidence

ORD record
ord-4bb38c44d1724fd6aba570a5c3f4a0b0
Source dataset
uspto-grants-1978_05
Patent number
US04091107

Reaction notes

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