HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethyl 7-(methanesulfinamido)heptanoate → ethyl 7-[N-(4-acetoxy-(E)-2-nonenyl)methanesulfonamido]heptanoic acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethyl 7-(methanesulfinamido)heptanoate | HCID 20327657 | — |
| Reactant | ethyl 7-[N-(4-acetoxynonyl)methanesulfinamido]heptanoate | HCID 20327711 | — |
| Reactant | Methanesulfonamido heptanoate | HCID 86735728 | — |
| Product | ethyl 7-[N-(4-acetoxy-(E)-2-nonenyl)methanesulfonamido]heptanoic acid | HCID 20327696 | — |
Reaction Steps
The synthesis of this compound is carried out as described in Example 1 except that, in Step A, the ethyl 7-(methanesulfonamido heptanoate is replaced by an equimolar amount of ethyl 7-(methanesulfinamido)heptanoate (Example T). The product of Step A is thus ethyl 7-[N-(4-acetoxynonyl)methanesulfinamido]heptanoate. The subsequent step yields 7-[N-(4-hydroxynonyl)methanesulfinamido]heptanoic acid (B).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04091107 |
| Source dataset | uspto-grants-1978_05 |
| ORD ID | ord-89047b3fdc17496cb5c225c1e7bdfab1 |
| Source note | uspto-grants-1978_05 |