HuagongsheHuagongshe Chemistry Print Report · For research reference only
ethyl 7-{N-[3-(1-acetoxycyclohexyl)-2-propynyl]methanesulfonamido}heptanoate → 7-{N-[3-(1-Hydroxycyclohexyl)propyl]methanesulfonamido}heptanoic Acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | ethyl 7-{N-[3-(1-acetoxycyclohexyl)-2-propynyl]methanesulfonamido}heptanoate | HCID 20327718 | — |
| Reactant | 1-bromo-4(R)-acetoxy-2-nonyne | HCID 22793816 | — |
| Reactant | 1-Acetoxy-1-(3-bromo-1-propynyl)cyclohexane | HCID 23339581 | — |
| Product | 7-{N-[3-(1-Hydroxycyclohexyl)propyl]methanesulfonamido}heptanoic Acid | HCID 20327665 | — |
Reaction Steps
The synthesis of this compound is carried out as described in Example 3 except that, in Step A, the 1-bromo-4(R)-acetoxy-2-nonyne is replaced by an equimolar amount of 1-acetoxy-1-(3-bromo-1-propynyl)cyclohexane (Example U). The product of Step A is thus ethyl 7-{N-[3-(1-acetoxycyclohexyl)-2-propynyl]methanesulfonamido}heptanoate.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04091107 |
| Source dataset | uspto-grants-1978_05 |
| ORD ID | ord-b306c76853914eba824288680a9d317f |
| Source note | uspto-grants-1978_05 |