HuagongsheHuagongshe Chemistry Print Report · For research reference only
Aniline → 1,1'-(Phenylimino)bis[3-chloro-2-propanol]
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Aniline | HCID 6115 | — |
| Reactant | Epichlorohydrin | HCID 7835 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | 1,1'-(Phenylimino)bis[3-chloro-2-propanol] | HCID 13479414 | 75% |
Reaction Steps
1.0 mol of aniline and 2.4 mol of epichlorohydrin are heated in 375 ml of ethanol for 16 h under reflux. The solvent is then removed in vacuum and the residue introduced drop by drop into n-hexane. The crystals obtained are filtered off and dried (yield: 75%); MP: 60° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05420172 |
| Source dataset | uspto-grants-1995_05 |
| ORD ID | ord-681234080a8d4959b6efe0b4667aeb7b |
| Source note | uspto-grants-1995_05 |