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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 373136Generated: October 25, 2026

Benzoic Acid → 6-Benzoylbenzothiazolinone

https://huagongshe.com/reaction/373136

Reaction equation

Participants

RoleNameHCIDCharge
ReactantBenzoic AcidHCID 243—
ReactantBenzothiazolinoneHCID 53400715—
Product6-BenzoylbenzothiazolinoneHCID 131717159—

Reaction Conditions

Temperature130 °C

Reaction Steps

To a solution of 0.04 mol of benzothiazolinone in 150 g of polyphosphoric acid there is slowly added, with agitation, 0.05 mol of benzoic acid. The reaction medium is heated to 130° C. for 4 hours. After cooling, the mixture is hydrolyzed in 10 volumes of ice-cold water.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS05162350
Source datasetuspto-grants-1992_11
ORD IDord-a31a0d9e825f49969fca7802ab029d5e
Source noteuspto-grants-1992_11