6-Benzoylbenzothiazolinone → 6-[1-Hydroxypentyl]Benzothiazolinone

HRID 373141Notes

Reaction equation

[C:1]([C:9]1[CH:18]=[CH:17][C:12]2[N:13]=[CH:14][S:15](=[O:16])[C:11]=2[CH:10]=1)(=[O:8])[C:2]1C=C[CH:5]=[CH:4][CH:3]=1.C(C1C=CC2N=CS(=O)C=2C=1)(=O)CCCC>>[OH:8][CH:1]([C:9]1[CH:18]=[CH:17][C:12]2[N:13]=[CH:14][S:15](=[O:16])[C:11]=2[CH:10]=1)[CH2:2][CH2:3][CH2:4][CH3:5]

Participants

Reactant 2

HCID 1317171596-Benzoylbenzothiazolinone

HCID 1317176266-Valerylbenzothiazolinone

Product 1

HCID 1317176256-[1-Hydroxypentyl]Benzothiazolinone

Procedure

The procedure is as in Example 28, but replacing the 6-benzoyl benzothiazolinone by the 6-valerylbenzothiazolinone obtained in Example 9. The agitation is maintained for 48 hours.

Workup

temperatureThe agitation is maintained for 48 hours

Sources & evidence

ORD record: ord-46893e4c127f42f8ba43c2da4a02d46d
Source dataset: uspto-grants-1992_11
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US05162350

Reaction notes

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