HuagongsheHuagongshe Chemistry Print Report · For research reference only
Propylene Oxide → Acryloylglycine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Propylene Oxide | HCID 6378 | — |
| Reactant | Potassium Hydroxide | HCID 14797 | — |
| Reactant | Sodium Pyrrolidone Carboxylate | HCID 23666346 | — |
| Solvent | Water | HCID 962 | — |
| Product | Acryloylglycine | HCID 100321 | 292.6% |
Reaction Steps
100 g of 25 wt % polyacrylic acid aqueous solution and 2.5 g of N-carboxy methyl acrylamide were polymerized at 60° C. for 3 hours for partial crosslinking. Potassium hydroxide was added to neutralize the pH value to 7.0 and 40 g of T-P400(polymer of triol and propylene oxide, Union Carbide Co., U.S.A.) and 1 g of sodium 2-pyrrolidone-5-carboxylate were added. Deionized water was then added to the resultant product to adjust the solid content thereof to 35 wt %. The viscosity of the resultant solution was measured as 5500 to 6000 cps(30° C.). The resulting product was tested according to the procedures set forth in Example 1, and the test results are listed in Table 1.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05420182 |
| Source dataset | uspto-grants-1995_05 |
| ORD ID | ord-6090913c96ce484f959002b7770a8a83 |
| Source note | uspto-grants-1995_05 |