Dodecanoyl chloride → N-[2-(2-hydroxyethyl)aminoethyl]-N-(2-hydroxyethyl) dodecanamide

HRID 373195Notes

Reaction equation

[OH:1][CH2:2][CH2:3][NH:4][CH2:5][CH2:6][NH:7][CH2:8][CH2:9][OH:10].[C:11](Cl)(=[O:23])[CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH3:22]>>[OH:1][CH2:2][CH2:3][NH:4][CH2:5][CH2:6][N:7]([CH2:8][CH2:9][OH:10])[C:11](=[O:23])[CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH3:22]

Participants

Reactant 2

HCID 8166Dodecanoyl chloride

HCID 78179Ethanol, 2,2'-(1,2-ethanediyldiimino)bis-

Product 1

HCID 14367842N-[2-(2-hydroxyethyl)aminoethyl]-N-(2-hydroxyethyl) dodecanamide

Procedure

5.3 g of N,N'-Bis(2-hydroxyethyl)ethylenediamine and 3.0 g of dodecanoyl chloride were reacted together following the procedure under Example 3. This provided 3.3 g of pure product, m.p. 94° C.

Sources & evidence

ORD record: ord-7b10bcd4526045df8c3d7369c0490aab
Source dataset: uspto-grants-1992_11
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US05162315

Reaction notes

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