1-(2-Hydroxyethyl)piperazine → HCID 19811297, compound

HRID 373196Notes

Reaction equation

[OH:1][CH2:2][CH2:3][N:4]1[CH2:9][CH2:8][NH:7][CH2:6][CH2:5]1.[C:10](Cl)(=[O:22])[CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH3:21]>>[O:22]=[C:10]([N:7]1[CH2:8][CH2:9][N:4]([CH2:3][CH2:2][OH:1])[CH2:5][CH2:6]1)[CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH3:21]

Participants

Reactant 2

HCID 76771-(2-Hydroxyethyl)piperazine

HCID 8166Dodecanoyl chloride

Product 1

HCID 19811297HCID 19811297, compound

Procedure

5.2 g of 1-(2-hydroxyethyl)piperazine and 8.8 g of dodecanoyl chloride was reacted following the procedure under Example 3. This provided 8.7 g of product, m.p. 38°-40° C.

Sources & evidence

ORD record: ord-1f78d44c89bc47099398140b2bd3e513
Source dataset: uspto-grants-1992_11
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US05162315

Reaction notes

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