m-Chloroperbenzoic acid → HCID 19811516, compound

Participants

Reaction Steps

To a solution of 3-propyl-6-propylthio-1-[[2'-(N-trityltetrazol-5-yl)biphenyl-4-yl]methyl]pyrimidine-2,4(1H,3H)-dione (0.6 g) in dichloromethane (10 ml) was added m-chloroperbenzoic acid (0.16 g) and the mixture was stirred at room temperature for 16 hours. The reaction mixture was washed with an aqueous sodium bicarbonate solution and water, and evaporated to dryness. The resulting residue was purified by column chromatography on silica gel to give colorless powders (0.27 g, 44%).

Provenance & Evidence