Boron trifluoride etherate → HCID 15156775, compound

HRID 373319Notes

Reaction equation

HRID 373319 reaction equation
[CH3:1][O:2][CH:3](OC)[CH2:4][NH:5][C:6](=[S:15])[S:7][CH2:8][C:9]1[CH:14]=[CH:13][CH:12]=[CH:11][N:10]=1.FB(F)F.CCOCC>>[CH3:1][O:2][CH:3]1[S:15][C:6]([S:7][CH2:8][C:9]2[CH:14]=[CH:13][CH:12]=[CH:11][N:10]=2)=[N:5][CH2:4]1

Participants

3

Reactant 2

HCID 8000Boron trifluoride etherateHCID 15156768HCID 15156768, compound

Product 1

HCID 15156775HCID 15156775, compoundYield 97%

Procedure

68.1 g (0.025 mole) of dithiocarbamate (VI) obtained from Example 7 was reacted with 8.51 g (0.06 mole) of trifluoroborane ether according to the same procedure as that in Example 9-2 to obtain 5.82 g (yield 97%) of the desired thiazoline compound.

Sources & evidence

ORD record
ord-b4998eee015448a680d1b3ff6f285954
Source dataset
uspto-grants-1992_11
Patent number
US05162534

Reaction notes

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