Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Citric Acid | HCID 311 | — |
| Reactant | Glyoxylylspermidine | HCID 133564 | — |
| Reactant | HCID 178479429 | HCID 178479429 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 178512808 | HCID 178512808 | — |
Reaction Steps
A mixture of 10.0 g (45.0 m moles) of 7-guanidinoheptanamide hydrochloride, 13.1 g (45.0 moles) of N-[4-(3-aminopropyl)aminobutyl]-2,2-dihydroxyethanamide dihydrochloride, and 3.2 g (15 m moles) of citric acid in water (100 ml) was evaporated to dryness to give a syrup which contained 1.0 g of water. The resulting syrup was heated at 60° C. for 8 hours.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US05162581 |
|---|
| Source dataset | uspto-grants-1992_11 |
|---|
| ORD ID | ord-cab24a28696d4348b9815b96e24e4dba |
|---|
| Source note | uspto-grants-1992_11 |
|---|
