HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethyl Acrylate → Ethyl 3-(m-bromophenoxy)propionate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethyl Acrylate | HCID 8821 | — |
| Reactant | 3-Bromophenol | HCID 11563 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | Ethyl 3-(m-bromophenoxy)propionate | HCID 19935504 | 52.9% |
Reaction Steps
A mixture of 20 g of 3-bromophenol, 92 g of ethyl acrylate and 1.8 ml of Triton B (35% in methanol) was boiled at reflux overnight. After distilling off the excess acrylate at normal pressure, the residue was distilled in a high vacuum. There were obtained 16.7 g of ethyl 3-(m-bromophenoxy)propionate as a colorless oil, boiling point 107°-110° C./67 Pa.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05164387 |
| Source dataset | uspto-grants-1992_11 |
| ORD ID | ord-6c798ae7750542b1a7a51eb6b65203cb |
| Source note | uspto-grants-1992_11 |