HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Cyclopropyl-6,7-difluoro-1,4-dihydro-4-oxoquinoline-3-carboxylic acid → HCID 20089993, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Cyclopropyl-6,7-difluoro-1,4-dihydro-4-oxoquinoline-3-carboxylic acid | HCID 5210422 | — |
| Reactant | tert-Butyl 3-azabicyclo[4.1.0]heptan-1-ylcarbamate | HCID 20089946 | — |
| Product | HCID 20089993 | HCID 20089993 | 65% |
Reaction Steps
According to the procedure of Example 34A, 1-tertbutoxycarbonylamino-3-azabicyclo[4.1.0]heptane (270.0 mg, 1.27 mmol) and 1-cyclopropyl-6,7-difluoro-1,4-dihydro-4-oxo-quinoline-3-carboxylic acid (275.6 mg, 1.03 mmol) were reacted to generate the title compound (304.2 mg, 0.666 mmol, 65%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05164402 |
| Source dataset | uspto-grants-1992_11 |
| ORD ID | ord-a9d5859a8afe490fafc2815b8b41a841 |
| Source note | uspto-grants-1992_11 |