Palladium → HCID 86746347, compound

HRID 373752Notes

Reaction equation

HRID 373752 reaction equation
[Pd].[Cl:2][Pd:3][Cl:4].[S:5]([CH2:9][CH2:10][CH2:11][N:12]1[CH:17]=[CH:16][CH:15]=[CH:14][CH2:13]1)([OH:8])(=[O:7])=[O:6]>O.C(O)C>[Pd:3]([Cl:4])[Cl:2].[S:5]([CH2:9][CH2:10][CH2:11][N:12]1[CH:13]=[CH:14][CH:15]=[CH:16][CH2:17]1)([OH:8])(=[O:6])=[O:7].[S:5]([CH2:9][CH2:10][CH2:11][N:12]1[CH:13]=[CH:14][CH:15]=[CH:16][CH2:17]1)([OH:8])(=[O:6])=[O:7].[S:5]([CH2:9][CH2:10][CH2:11][N:12]1[CH:13]=[CH:14][CH:15]=[CH:16][CH2:17]1)([OH:8])(=[O:6])=[O:7].[S:5]([CH2:9][CH2:10][CH2:11][N:12]1[CH:13]=[CH:14][CH:15]=[CH:16][CH2:17]1)([OH:8])(=[O:6])=[O:7]

Participants

6

Reactant 3

HCID 23938PalladiumHCID 24290Palladium ChlorideHCID 19808197HCID 19808197, compound

Product 1

HCID 86746347HCID 86746347, compound

Reagents, catalysts & solvents 2

HCID 702EthanolSolventHCID 962WaterSolvent

Procedure

250 mg of palladium in the form of PdCl2 are reacted under stirring with 1-(3-sulfopropyl)pyridine, in a molar ratio from 1 to 4, at 50° for 20 minutes, in 500 ml of water and 500 ml of ethyl alcohol.

Sources & evidence

ORD record
ord-1d9e850f09d3409689a934ab40192325
Source dataset
uspto-grants-1992_11
Patent number
US05165971

Reaction notes

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