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Acetic Acid → 4-(4-(2-Quinolinylmethylsulfonyl)styryl)benzoic acid
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Acetic Acid | HCID 176 | — |
| 反応物 | Hydrogen Peroxide | HCID 784 | — |
| 反応物 | 4-(4-(2-Quinolinylmethylsulfinyl)styryl)benzoic acid | HCID 54512756 | — |
| 溶媒 | Dichloromethane | HCID 6344 | — |
| 生成物 | 4-(4-(2-Quinolinylmethylsulfonyl)styryl)benzoic acid | HCID 54457133 | — |
反応手順
To 3 mmol of the sulfinyl compound from Step A in acetic acid (40 mmol) is added 30% hydrogen peroxide (2 ml). The mixture is stirred at ambient temperature and assayed by TLC. Upon disappearance of the sulfinyl starting compound, the reaction mixture is diluted with dichloromethane, washed with dilute aqueous sodium bisulfite and water, dried and evaporated to give 4-(4-(2-quinolinylmethylsulfonyl)styryl)benzoic acid.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05166210 |
| 出典データセット | uspto-grants-1992_11 |
| ORD ID | ord-01cf7ebcee884278be3216537458d942 |
| 出典メモ | uspto-grants-1992_11 |