HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimethylformamide → HCID 86746383, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimethylformamide | HCID 6228 | — |
| Reactant | Oxalyl chloride | HCID 65578 | — |
| Reactant | HCID 86746382 | HCID 86746382 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 86746383 | HCID 86746383 | 99% |
Reaction Steps
To a mixture of 7.0 g (0.0336 mol) of cis-3-(benzoylthio)propenoic acid and 0.5 ml of N,N-dimethylformamide in 100 ml of dichloromethane under nitrogen was added 2.93 ml (0.0336 mol) of oxalyl chloride. After 12 h the solvents were removed to give 7.5 g (99% yield) of cis-3-(benzoylthio)propenoyl chloride as a pale yellow solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05166390 |
| Source dataset | uspto-grants-1992_11 |
| ORD ID | ord-b52a30aead7c415db5c945d4525706be |
| Source note | uspto-grants-1992_11 |