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HRID374311

反应详情

EQUATION

反应方程式

HRID 374311 的结构方程式

REACTANTS

反应物

1
结构：O=C(O)[C@H](Cc1ccccc1)C[C@@H](Cc1ccccc1)C(=O)O
HCID14557654

未命名化合物

PRODUCTS

生成物

1
结构：O=C1OC(=O)[C@H](Cc2ccccc2)C[C@H]1Cc1ccccc1
HCID14557658

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CC(=O)Cl
溶剂HCID6367

Acetyl chloride

C2H3ClO

PROCEDURE

实验过程

The (S,S)-2,4-dibenzylglutaric anhydride [mp 172°-174°; [alpha]D =-19.1° (c=1 in CHCl3)] is prepared similarly by refluxing (S,S)-2,4-dibenzylglutaric acid in acetyl chloride for 3 hours, concentrating the mixture and recrystallizing from toluene.

WORKUP

后处理

  1. concentrationconcentrating the mixture
  2. customrecrystallizing from toluene