HuagongsheHuagongshe Chemistry Print Report · For research reference only
Stearic Acid → 1-Chlorooctadecane
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Stearic Acid | HCID 5281 | — |
| Reactant | Phosgene | HCID 6371 | — |
| Product | 1-Chlorooctadecane | HCID 18815 | 99.9% |
Reaction Steps
The experimental method described in Example 1 is used, and 2,746 g (10 moles) of technical grade stearic acid and the catalyst phase (342 g) obtained in Example 1 are initially taken. 1,089 g (11 moles) of gaseous phosgene are then introduced. The product phase contains 2,930 g (99.9% yield) of stearyl chloride having a purity of 97% (determined by IR spectroscopy); the iodine color number is 30.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05166427 |
| Source dataset | uspto-grants-1992_11 |
| ORD ID | ord-036e48ed98a246a49a6fe4680c24cf33 |
| Source note | uspto-grants-1992_11 |