2,4-Difluorophenyl isocyanate → 1,4-Bis[[1-heptyl-3-(2,4-difluorophenyl)ureido]methyl]benzene

Participants

Reaction Steps

To a solution of 1.5 g N,N'-diheptyl-p-xylylenediamine in 20 ml n-hexane, was added dropwise with stirring 5 ml of a n-hexane solution containing 1.4 g 2,4-difluorophenyl isocyanate under ice cooling. Stirring was continued at room temperature for two hours, and the solid which separated out was collected by filtration and recrystallized from methanol, giving 2.3 g of 1,4-bis[[1-heptyl-3-(2,4-difluorophenyl)ureido]methyl]benzene.

Provenance & Evidence