HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methanesulfonic Acid → 1-Methyl-2-isopropylamino-5-methoxycarbonylpyrimidinium sulfate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methanesulfonic Acid | HCID 6395 | — |
| Reactant | 1-Methyl-2-isopropylamino-5-methoxycarbonylpyrimidinium hydroxide | HCID 19698816 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | 1-Methyl-2-isopropylamino-5-methoxycarbonylpyrimidinium sulfate | HCID 67660295 | — |
Reaction Steps
1.09 mlg [sic] (16.78 mol; 1.61 g) of methanesulfonic acid is added to a solution of 1-methyl-2-isopropylamino-5-methoxycarbonylpyrimidinium hydroxide (3.48 g; 15.35 mol) dissolved in 100 ml of anhydrous tetrahydrofuran. The mixture is stirred under argon at room temperature for one hour. The precipitate which forms is filtered and then rinsed with ether.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05480884 |
| Source dataset | uspto-grants-1996_01 |
| ORD ID | ord-c030ad34ab36425c8415fa7c69c341ec |
| Source note | uspto-grants-1996_01 |