HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrogen Bromide → 3-(3-Bromopropyl)pyridine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrogen Bromide | HCID 260 | — |
| Reactant | 3-Pyridinepropanol | HCID 17861 | — |
| Product | 3-(3-Bromopropyl)pyridine | HCID 12701568 | — |
Reaction Steps
To 17.0 g (124 moles) of 3-(3-pyridyl)-1-propanol was added 240 mL of 48% hydrobromic acid. The mixture was heated under reflux for 4 hours, and then evaporated to dryness to afford the hydrobromide salt of 3-(3-pyridyl)-1-bromopropane as an oil in quantitative yield.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05480892 |
| Source dataset | uspto-grants-1996_01 |
| ORD ID | ord-d62f1374cf5c45a8a395275ffd52cb2d |
| Source note | uspto-grants-1996_01 |