HCID 15286101, compound → HCID 54464555, compound

HRID 374504Notes

Reaction equation

HRID 374504 reaction equation
[C:1]1([CH3:23])[CH:6]=[CH:5][C:4]([N:7]2[CH2:11][CH:10]([CH2:12][O:13][C:14]3[CH:21]=[CH:20][C:17]([CH:18]=[O:19])=[CH:16][CH:15]=3)[O:9][C:8]2=[O:22])=[CH:3][CH:2]=1.ClC1C=CC(N2CC(COC3C=CC(C=O)=CC=3)OC2=O)=CC=1>>[C:1]1([CH3:23])[CH:2]=[CH:3][C:4]([N:7]2[CH2:11][CH:10]([CH2:12][O:13][C:14]3[CH:21]=[CH:20][C:17]([CH2:18][OH:19])=[CH:16][CH:15]=3)[O:9][C:8]2=[O:22])=[CH:5][CH:6]=1

Participants

3

Reactant 2

HCID 15286101HCID 15286101, compoundHCID 15286112HCID 15286112, compound2×

Product 1

HCID 54464555HCID 54464555, compoundYield 63%

Procedure

The same procedure of Example 20 was repeated except that 4-[3-(4-tolyl)-2-oxooxazolidin-5-yl]methoxybenzaldehyde (compound 20) obtained in Example 2 was used in lieu of 4-[3-(4-chlorophenyl)-2-oxooxazolidin-5-yl]methoxybenzaldehyde to give the title compound (compound 175) in a yield of 63%.

Workup

  1. customobtained in Example 2

Sources & evidence

ORD record
ord-487977137dc44893a9cc422d2ac1b093
Source dataset
uspto-grants-1996_01
Patent number
US05480899

Reaction notes

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