HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 57129233, compound → HCID 22844605, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 57129233 | HCID 57129233 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 22844605 | HCID 22844605 | 101.8% |
Reaction Steps
70 mg of (4S,5RS)-3-benzyloxycarbonyl-4-cyclohexylmethyl-2,2-dimethyl-5-[(1RS)-1-hydroxy-2-(4methylpiperidino)ethyl]oxazolidine was dissolved in 1.5 ml of ethanol, and palladium black was added thereto. The mixture was treated in the same manner as in Example 17 to obtain 45 mg of (2RS,3RS,4S)-4-amino-5-cyclohexyl-1-(4-methylpiperidino)-2,3-pentanediol as colorless oily substance.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05481036 |
| Source dataset | uspto-grants-1996_01 |
| ORD ID | ord-52509ea524a14c0db083de49ab46aacc |
| Source note | uspto-grants-1996_01 |