HuagongsheHuagongshe Chemistry Print Report · For research reference only
3,4-Dinitrotoluene → 3,4-Dinitrobenzaldehyde
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3,4-Dinitrotoluene | HCID 11883 | — |
| Reactant | N-bromobutanimide | HCID 67184 | — |
| Catalyst | Tungsten | HCID 23964 | — |
| Solvent | Carbon Tetrachloride | HCID 5943 | — |
| Product | 3,4-Dinitrobenzaldehyde | HCID 3362201 | — |
Reaction Steps
One equivalent of 3,4-dinitrotoluene and 2 equivalents of N-bromosuccinimide in carbon tetrachloride is irradiated with a 500 W tungsten lamp for 4 hours. The mixture is filtered and the filtrated is shaken with a solution of aqueous potassium carbonate. The organic layer is evaporated in vacuo to give 3,4-dinitrobenzaldehyde.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05482971 |
| Source dataset | uspto-grants-1996_01 |
| ORD ID | ord-11da24e3853b4b24b0cdb559065cb01c |
| Source note | uspto-grants-1996_01 |