HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Benzoyl-4,5-dichlorobenzoic acid → HCID 21463235, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Benzoyl-4,5-dichlorobenzoic acid | HCID 12205291 | — |
| Reactant | HCID 15214193 | HCID 15214193 | — |
| Product | HCID 21463235 | HCID 21463235 | — |
Reaction Steps
2-Benzoyl-4,5-dichlorobenzoic acid, in place of 2-benzoyl-4,5-dimethylbenzoic acid, was reacted and treated in the same manner as in Process 1 of Reference Example 29 to yield 6,7-dichloro-4-phenylisocoumarin-3-carboxylic acid [melting point 243°-244° C. (recrystallized from ethyl acetate-isopropyl ether)]. This compound was reacted and treated in the same manner as in Process 2 of Reference Example 29 to yield the title compound as colorless crystals.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05482967 |
| Source dataset | uspto-grants-1996_01 |
| ORD ID | ord-53a6894e84a04833aaf2d9e61779833a |
| Source note | uspto-grants-1996_01 |