HuagongsheHuagongshe Chemistry Print Report · For research reference only
Butylbenzene → HCID 23513091, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Butylbenzene | HCID 7705 | — |
| Reactant | Glyoxal, phenyl-, hydrate | HCID 12215922 | — |
| Catalyst | Titanium Tetrachloride | HCID 24193 | — |
| Solvent | 1,1-Dichloroethane | HCID 6365 | — |
| Product | HCID 23513091 | HCID 23513091 | — |
Reaction Steps
Phenylglyoxal monohydrate (304 mg, 2 mM) and n-butylbenzene (0.62 ml, 4 mM) were dissolved in dichloroethane (4 ml), titanium tetrachloride (0.33 ml, 3 mM) was added, and reacted at room temperature for 1 hour. Using the same procedure as in Example 1, 4'-n-butylbenzoin was obtained as crystal (362.7 mg, 67.2% yield).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05484689 |
| Source dataset | uspto-grants-1996_01 |
| ORD ID | ord-826006f52bb345a79b0a2c9be445972e |
| Source note | uspto-grants-1996_01 |