反应详情

Phenylglyoxal monohydrate (304 mg, 2 mM) and n-heptylbenzene (0.82 ml, 4 mM) were dissolved in dichloroethane (3 ml), titanium tetrachloride (0.33 ml, 3 mM) was added, and reacted at room temperature for 1 hour. Using the same procedure as in Example 1, 4'-n-heptylbenzoin was obtained as crystal (386.7 mg, 61.5% yield).

1. customreacted at room temperature for 1 hour