HuagongsheHuagongshe Chemistry Print Report · For research reference only
Octylbenzene → HCID 13742410, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Octylbenzene | HCID 16607 | — |
| Reactant | Glyoxal, phenyl-, hydrate | HCID 12215922 | — |
| Catalyst | Titanium Tetrachloride | HCID 24193 | — |
| Solvent | 1,1-Dichloroethane | HCID 6365 | — |
| Product | HCID 13742410 | HCID 13742410 | — |
Reaction Steps
Phenylglyoxal monohydrate (608 mg, 4 mM) and n-octylbenzene (1.77 ml, 8 mM) were dissolved in dichloroethane (8 ml), titanium tetrachloride (0.66 ml, 6 mM) was added, and reacted at room temperature for 30 minutes. Using the same procedure as in Example 1, 4'-n-octylbenzoin was obtained as crystal (810.0 mg, 62.6% yield).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05484689 |
| Source dataset | uspto-grants-1996_01 |
| ORD ID | ord-7915a95a149c4f35a700216a2be8fa61 |
| Source note | uspto-grants-1996_01 |