HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimethyl Sulfoxide → 2-(1-(Benzyloxyamino)ethyl)benzo[b]thiophene
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimethyl Sulfoxide | HCID 679 | — |
| Reactant | O-Benzylhydroxylamine | HCID 102313 | — |
| Reactant | 2-(1-Chloroethyl)benzo[b]thiophene | HCID 18779254 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | 2-(1-(Benzyloxyamino)ethyl)benzo[b]thiophene | HCID 19935888 | — |
Reaction Steps
heating 2-(1-chloroethyl)benzo[b]thiophene with O-benzylhydroxylamine in a solvent such as dimethyl sulphoxide or tetrahydrofuran to give 2-(1-(benzyloxyamino)ethyl)benzo[b]thiophene of formula: ##STR4##
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05420300 |
| Source dataset | uspto-grants-1995_05 |
| ORD ID | ord-00f36ee121f6420c94f2834e54e0d4f7 |
| Source note | uspto-grants-1995_05 |