Methyl iodide → HCID 20152992, compound

HRID 3752Notes

Reaction equation

[Cl:1][C:2]1[C:7]([NH:8][S:9]([C:12]2[N+:13]([O-:18])=[CH:14][CH:15]=[CH:16][CH:17]=2)(=[O:11])=[O:10])=[CH:6][CH:5]=[CH:4][N:3]=1.[CH3:19]I>>[CH3:19][N:8]([C:7]1[C:2]([Cl:1])=[N:3][CH:4]=[CH:5][CH:6]=1)[S:9]([C:12]1[N+:13]([O-:18])=[CH:14][CH:15]=[CH:16][CH:17]=1)(=[O:10])=[O:11]

Participants

Reactant 2

HCID 6328Methyl iodide

HCID 20152990HCID 20152990, compound

Product 1

HCID 20152992HCID 20152992, compound

Procedure

The title compound of Example 5 above is reacted with methyl iodide (0.6 g, 0.26 ml, 4.2 mmol) to give N-methyl-N-(2-chloro-3-pyridyl)-2-pyridinesulfonamide 1-oxide, MS m/e 300.00 (M+ +1).

Sources & evidence

ORD record: ord-a21c399ab50c44979c3f814313d13bd3
Source dataset: uspto-grants-1988_02
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US04722749

Reaction notes

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