戻る
化工社化工社 化学情報印刷レポート · 研究参考用
HRID 375295作成日:2026年10月25日

5,6-Diamino-1,3-diethyluracil → 1H-Purine-2,6-dione, 3,7-dihydro-1,3-diethyl-8-(2-(2,3-dimethyl-4-methoxy)phenyl)ethenyl)-, (E)-

https://huagongshe.com/reaction/375295

反応式

関与物質

役割名称HCID仕込み量
反応物5,6-Diamino-1,3-diethyluracilHCID 4572133—
反応物4-Methoxy-2,3-dimethylcinnamic acidHCID 53401770—
生成物1H-Purine-2,6-dione, 3,7-dihydro-1,3-diethyl-8-(2-(2,3-dimethyl-4-methoxy)phenyl)ethenyl)-, (E)-HCID 6448857—

反応手順

Substantially the same procedure as in Example 7 was repeated using 2.5 g (12.6 mmol) of 5,6-diamino-1,3-diethyluracil and 2.9 g (13.9 mmol) of 4-methoxy-2,3-dimethylcinnamic acid. Then, the resultant crude crystals were recrystallized from ethanol/water to give 0.80 g (yield of Compound 72 as white crystals.

情報源と証拠

DOI10.6084/m9.figshare.5104873.v1
特許番号US05484920
出典データセットuspto-grants-1996_01
ORD IDord-87dc8dc2faf64499a136372f41208257
出典メモuspto-grants-1996_01