HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
2-Propenoic acid, 3-(3-methoxyphenyl)- → 1H-Purine-2,6-dione, 3,7-dihydro-1,3-diethyl-8-(2-(3-methoxyphenyl)ethenyl)-, (E)-
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 2-Propenoic acid, 3-(3-methoxyphenyl)- | HCID 87155 | — |
| Edukt | 5,6-Diamino-1,3-diethyluracil | HCID 4572133 | — |
| Produkt | 1H-Purine-2,6-dione, 3,7-dihydro-1,3-diethyl-8-(2-(3-methoxyphenyl)ethenyl)-, (E)- | HCID 6448878 | 49% |
Reaktionsschritte
Substantially the same procedure as in Example 7 was repeated using 2.50 g (12.6 mmol) of 5,6-diamino-1,3-diethyluracil and 2.48 g (13.9 mmol) of 3-methoxycinnamic acid. Then, the resultant crude crystals were recrystallized from dimethylformamide/water to give 2.10 g (yield 49%) of Compound 102 as a white powder.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US05484920 |
| Quelldatensatz | uspto-grants-1996_01 |
| ORD ID | ord-a64881f6b13a4e1db7a24285ca6df993 |
| Quellennotiz | uspto-grants-1996_01 |