HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 3891318, compound → (E)-1,3-Dipropyl-8-(2-(4-propoxyphenyl)ethenyl)-3,7-dihydro-1H-purine- 2,6-dione
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 3891318 | HCID 3891318 | — |
| Reactant | 5,6-Diamino-1,3-dipropyl-2,4(1H,3H)-pyrimidinedione | HCID 5098605 | — |
| Product | (E)-1,3-Dipropyl-8-(2-(4-propoxyphenyl)ethenyl)-3,7-dihydro-1H-purine- 2,6-dione | HCID 6448797 | 33% |
Reaction Steps
Substantially the same procedure as in Reference Example 1 was repeated using 3.0 g (13.3 mmol) of 5,6-diamino-1,3-dipropyluracil and 3.01 g (14.6 mmol) of 4-propoxycinnamic acid. Then, the resultant crude crystals were recrystallized from dioxane/water to give 1.71 g (yield 33%) of Compound 49 as pale brown needles.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05484920 |
| Source dataset | uspto-grants-1996_01 |
| ORD ID | ord-8bdb520d987147f78422dfaa72a25a24 |
| Source note | uspto-grants-1996_01 |