HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-(3-Bromo-4-methoxyphenyl)-2-propenoic acid → 151539-48-9
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-(3-Bromo-4-methoxyphenyl)-2-propenoic acid | HCID 719754 | — |
| Reactant | 5,6-Diamino-1,3-dipropyl-2,4(1H,3H)-pyrimidinedione | HCID 5098605 | — |
| Product | 151539-48-9 | HCID 6448801 | 58% |
Reaction Steps
Substantially the same procedure as in Reference Example 1 was repeated using 3.0 g (13.3 mmol) of 5,6-diamino-1,3-dipropyluracil and 3.75 g (14.6 mmol) of 3-bromo-4-methoxycinnamic acid. Then, the resultant crude crystals were recrystallized from dioxane to give 3.43 g (yield 58%) of Compound 55 as yellow needles.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05484920 |
| Source dataset | uspto-grants-1996_01 |
| ORD ID | ord-b570d8927b0049fbaa0b7c312c8a8b0a |
| Source note | uspto-grants-1996_01 |