HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 735099, compound → 151539-54-7
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 735099 | HCID 735099 | — |
| Reactant | 5,6-Diamino-1,3-dipropyl-2,4(1H,3H)-pyrimidinedione | HCID 5098605 | — |
| Product | 151539-54-7 | HCID 6448805 | 67% |
Reaction Steps
Substantially the same procedure as in Reference Example 1 was repeated using 1.5 g (6.64 mmol) of 5,6-diamino-1,3-dipropyluracil and 2.10 g (7.31 mmol) of 3-bromo-4,5-dimethoxycinnamic acid. Then, the resultant crude crystals were recrystallized from dioxane/water to give 2.11 g (yield 67%) of Compound 59 as white needles.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05484920 |
| Source dataset | uspto-grants-1996_01 |
| ORD ID | ord-fe498d04addb4392a05d16709120f7c3 |
| Source note | uspto-grants-1996_01 |