HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-(3,5-Dimethoxyphenyl)prop-2-enoic acid → 155271-60-6
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-(3,5-Dimethoxyphenyl)prop-2-enoic acid | HCID 86092 | — |
| Reactant | 5,6-Diamino-1,3-diethyluracil | HCID 4572133 | — |
| Product | 155271-60-6 | HCID 6448906 | 49% |
Reaction Steps
Substantially the same procedure as in Example 7 was repeated using 3.00 g (15.1 mmol) of 5,6-diamino-1,3-diethyluracil and 3.48 g (16.7 mmol) of 3,5-dimethoxycinnamic acid. Then, the resultant crude crystals were recrystallized from ethanol/water to give 2.74 g (yield 49%) of Compound 130 as a white powder.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05484920 |
| Source dataset | uspto-grants-1996_01 |
| ORD ID | ord-64e093b6a3ae42df8f2fc673bdc2df78 |
| Source note | uspto-grants-1996_01 |