HCID 18993322, compound → HCID 18993320, compound

HRID 375570Notes

Reaction equation

HRID 375570 reaction equation
[C:1]1([Li])[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.[CH3:8][O:9][C:10]1[CH:28]=[CH:27][C:13]([CH2:14][CH2:15][N:16]2[CH2:21][CH2:20][CH2:19][CH:18]([C:22]([O:24]CC)=O)[CH2:17]2)=[CH:12][CH:11]=1>>[C:1]1([C:22]([C:1]2[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=2)([OH:24])[CH:18]2[CH2:19][CH2:20][CH2:21][N:16]([CH2:15][CH2:14][C:13]3[CH:12]=[CH:11][C:10]([O:9][CH3:8])=[CH:28][CH:27]=3)[CH2:17]2)[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1

Participants

3

Reactant 2

HCID 18993322HCID 18993322, compoundHCID 178506676HCID 178506676, compound

Product 1

HCID 18993320HCID 18993320, compound

Procedure

The title compound was prepared by the method of Example 11 by reacting phenyllithium with ethyl 1-(4-methoxyphenethyl)piperidine-3-carboxylate. The title compound was obtained as a colourless oil.

Workup

  1. customThe title compound was prepared by the method of Example 11

Sources & evidence

ORD record
ord-f1dd8ea82b4b4a9097a4eddec7b59f29
Source dataset
uspto-grants-1996_01
Patent number
US05486527

Reaction notes

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