HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 18993315, compound → HCID 18993313, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 18993315 | HCID 18993315 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 18993313 | HCID 18993313 | 99.3% |
Reaction Steps
A solution of 3-diphenylmethylenepiperidine hydrochloride (200 mg, 0.7 mmol) in ethanol (40 ml) was stirred under one atmosphere of hydrogen at 40° C. in the presence of 10% palladium on charcoal (20 mg) for 24 hours and filtered. The filtrate was concentrated to give the title compound (200 mg) as a pale brown gum which was characterised by its 1H-NMR spectrum.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05486527 |
| Source dataset | uspto-grants-1996_01 |
| ORD ID | ord-6b6e82d3db554f89b44bcbb80cdaa98e |
| Source note | uspto-grants-1996_01 |