HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-[2-(4-Methoxyphenyl)ethenyl]-N,N-diphenylaniline → HCID 11211174, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-[2-(4-Methoxyphenyl)ethenyl]-N,N-diphenylaniline | HCID 53971508 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | 1,4-Dioxane | HCID 31275 | — |
| Product | HCID 11211174 | HCID 11211174 | — |
Reaction Steps
37.7 g (0.1 mol) of the 4-diphenylamino-4'-methoxystilbene prepared in Synthesis Example 1-1 was dissolved in 250 ml of dioxane. To the thus obtained mixture, 4 g of 5% Pd/C powder and then 2.4 l of hydrogen were added. A solvent was distilled away from the reaction mixture, whereby 1-(4-diphenylaminophenyl)-2-(4-methoxyphenyl)ethane was obtained as an oily transport compound of light yellow in color.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05488137 |
| Source dataset | uspto-grants-1996_01 |
| ORD ID | ord-40182713069e4e18b805074cef367777 |
| Source note | uspto-grants-1996_01 |