HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triacetoxyperiodinane → 5'-Formyl-5-methoxy-1,3,3-trimethylspiro[indoline-2,3'-[3H]-naphtho[2,1-b][1,4]oxazine]
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triacetoxyperiodinane | HCID 159087 | — |
| Reactant | 5'-hydroxymethyl-5-methoxy-1,3,3-trimethylspiro[indoline-2,3'-[3H]-naphtho[2,1-b][1,4]oxazine] | HCID 19360918 | — |
| Product | 5'-Formyl-5-methoxy-1,3,3-trimethylspiro[indoline-2,3'-[3H]-naphtho[2,1-b][1,4]oxazine] | HCID 15860297 | — |
Reaction Steps
This compound is prepared according to the method employed for Example 1, from 0.42 g (1 mmol) of Dess-Martin reactant and 0.39 g (1 mmol) of 5'-hydroxymethyl-5-methoxy-1,3,3-trimethylspiro[indoline-2,3'-[3H]-naphtho[2,1-b][1,4]oxazine].
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06019914 |
| Source dataset | uspto-grants-2000_02 |
| ORD ID | ord-f790a0036a2a4d8f93ab40f638bbd584 |
| Source note | uspto-grants-2000_02 |