HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethyl chloroformate → HCID 54540523, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethyl chloroformate | HCID 10928 | — |
| Reactant | HCID 69945842 | HCID 69945842 | — |
| Product | HCID 54540523 | HCID 54540523 | — |
Reaction Steps
The title carbamate was prepared as described in Example 88 from 436 mg (1.0 mmol) of the amidine from Example 69 and 119 mg (1.1 mmol) ethyl chloroformate. It was recrystallized from dichloromethane/hexane. Yield: 0.35 g (74%) of a white powder, m.p. 168-169° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06020362 |
| Source dataset | uspto-grants-2000_02 |
| ORD ID | ord-830868b2371f426aa3716fdc17dc3e74 |
| Source note | uspto-grants-2000_02 |