反应详情

温度

25 °C

In a 500-ml flask were placed 15 g of 2-methoxyacetophenone (made by Aldrich Co., 99% purity), 15 g of p-azidobenzaldehyde (manufactured by Kanto Chemical Co., Ltd.), 50 g of 10% aqueous solution of NaOH, and 50 g of methanol. The mixture was stirred in a yellow light at 25° C. for 24 hours. After completion of the reaction, the deposited crystals were filtered, washed with water, dried, and recrystallized from ethanol.

1. customIn a 500-ml flask were placed
2. customAfter completion of the reaction
3. filtrationthe deposited crystals were filtered
4. washwashed with water
5. customdried
6. customrecrystallized from ethanol