HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Pyrrolidone, 1-methyl- → 3-(3-Methyl-5-isoxazolyl)methylene-1-methylpiperidine oxalate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Pyrrolidone, 1-methyl- | HCID 144283 | — |
| Reactant | Isoxazole, 3-methyl-5-[(trimethylsilyl)methyl]- | HCID 10986681 | — |
| Reactant | HCID 70087037 | HCID 70087037 | — |
| Product | 3-(3-Methyl-5-isoxazolyl)methylene-1-methylpiperidine oxalate | HCID 70249731 | — |
Reaction Steps
3-(3-methyl-5-isoxazolyl)methylene-1-methylpyrolidine oxalate, compound 8, and (E) 3-(3-methyl-5-isoxazolyl)methylene-1-methylpyrrolidine oxalate, compound 9, starting form 1-methyl-pyrrolidin-3-one (J. Amer. Chem. Soc., 55, 1933, 1233-1241) and 3-methyl-5-trimethylsilylmethyl-isoxazole.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06022868 |
| Source dataset | uspto-grants-2000_02 |
| ORD ID | ord-48109cd8a4e949bdb140a50f345e55d4 |
| Source note | uspto-grants-2000_02 |